Chinese Journal of Applied Chemistry ›› 1993, Vol. 0 ›› Issue (2): 99-101.

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PREPARATION OF PbTiO3 POWDERS BY COPRECIPITATION METHOD

Zhao Zhenguo, Ma Jiming, Cheng Humin, Qiang Di   

  1. Department of Chemistry, Peking University, 100871 Beijing
  • Received:1992-04-20 Revised:1992-09-14 Published:1993-04-10 Online:1993-04-10

Abstract: The pure perovskite-lead titanate powders were prepared by coprecipitation method. The ethanol solution of the Ti(OC4H9)4 and methanol solution of the PbAc2 were mixed at a 1:1 molar ratio of Pb to Ti. Under intensive stiring the mixed solution was added dropwise to the water followed by adding H2O2 solution. The pH of the solution was adjusted to 8.9~9.2. by adding NH4OH. The resulted precipitate was washed with deionized water and then dried at 100℃. The dried material was pestled and calcined at temperature above 550℃ to yield PbTiO3 powders.

Key words: PbTiO3, powder, coprecipitation