Simultaneously Determining Thermal Decomposition Products of Pectin by a Combined Use of Simultaneous Thermal Analysis, FT-IR and GC-MS

doi:10.3724/SP.J.1095.2012.00572

Simultaneously Determining Thermal Decomposition Products of Pectin by a Combined Use of Simultaneous Thermal Analysis, FT-IR and GC-MS

LIU Chunbo¹, ZENG Xiaoying², WANG Kunmiao¹, ZHAO Wei¹, HAN Jingmei¹, HE Pei¹, CHEN Yongkuan1, MIAO Mingming¹, LIU Zhihua^1*

(1.Key Laboratory of Tobacco Chemistry of Yunnan,Yunnan Academy of Tobacco Science,Kunming 650106,China；
2.Technology Centre of Hongyun Honghe Tobacco(Group) Co.,Ltd,Kunming 650202,China)

Received:2011-12-27 Revised:2012-02-07 Published:2012-10-10 Online:2012-10-10

Abstract

Abstract: A combination system of simultaneous thermal analysis(STA), Fourier-transform infrared(FT-IR) spectroscopy and GC-MS was established for simultaneously determination of pyrolysised products of the pectin samples under nitrogen or nitrogen-oxygen atmosphere. According to the pyrolysis behavior of pectin, 26 substances were detected at three temperatures(243 ℃, 270 ℃ and 335 ℃) on line with the system.

Key words: STA, FT-IR, GC-MS, pectin pyrolysis

CLC Number:

O652

LIU Chunbo1, ZENG Xiaoying2, WANG Kunmiao1, ZHAO Wei1, HAN Jingmei1, HE Pei1, CHEN Yongkuan1, MIAO Mingming1, LIU Zhihua1*. Simultaneously Determining Thermal Decomposition Products of Pectin by a Combined Use of Simultaneous Thermal Analysis, FT-IR and GC-MS[J]. Chinese Journal of Applied Chemistry, DOI: 10.3724/SP.J.1095.2012.00572.

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Simultaneously Determining Thermal Decomposition Products of Pectin by a Combined Use of Simultaneous Thermal Analysis, FT-IR and GC-MS

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