中华医学超声杂志

应用化学 ›› 1995, Vol. 0 ›› Issue (5): 109-110.

• 研究论文 • 上一篇    下一篇

α－乙酰基硫代甲酰取代胺超声波辐射合成

方东1, 陈克潜2, 陆忠娥2, 孙大庆2   

  1. 1. 盐城师范专科学校科技部, 盐城 224002;
    2. 苏州大学化学系, 苏州
  • 收稿日期:1994-10-31 修回日期:1995-02-06 出版日期:1995-10-10 发布日期:1995-10-10

Synthesis of α-ACetylthioformanilides under Ultrasonic Irradiation

Fang Dong1, Chen Keqian2, Lu Zhonge2, Sun Daqing2   

  1. 1. Yancheng Teacher-training School, Yancheng 224002;
    2. Department of Chemistry, Suzhou University, Suzhou
  • Received:1994-10-31 Revised:1995-02-06 Published:1995-10-10 Online:1995-10-10

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摘要： a-羰基硫代酞胺与邻苯二胺、氨基脲、氨基硫脲反应可以生成某些具有生理活性的杂环化合物.由于a-羰基硫代酸胺的合成有一定难度,合成方法并不多.本文以a-乙酞基甲酞胺为原料,在超声波作用下进行硫代反应,合成了一系列a-乙酞基硫代酞胺类化合物.

关键词: 乙酰基硫代甲酰取代胺, 合成, 超声波辐射

Abstract: Some α-acetylthioformanilides have been svnthesized under ultrasonic irradiation.and the compounds have been confirmed by elemental analysis,IR and MS.The method issuperior in reaction velocity and yield.

Key words: acetylthioformanilide, synthesis, ultrasonic irradiation

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