中华医学超声杂志

应用化学 ›› 2010, Vol. 27 ›› Issue (02): 169-172.DOI: 10.3724/SP.J.1095.2010.90090

• 研究论文 • 上一篇    下一篇

芴三偶氮基水杨醛缩氨基芳基硫脲合成及其植物生长调节作用

冯驸1*,胡卫兵1,刘红霞2,聂响亮1,余爱农1   

  1. (1.湖北民族学院化学与环境工程学院 恩施 445000;
    2.黄石理工学院材料与工程学院 黄石)
  • 收稿日期:2009-02-10 修回日期:2009-06-23 出版日期:2010-02-10 发布日期:2010-02-10
  • 通讯作者: 冯驸，男，硕士，讲师; E-mail:fengfu04971118@yahoo.com.cn; 研究方向：有机合成
  • 基金资助:
    湖北省高等学校优秀中青年科技创新团队计划资助项目(T200707)

Study on the Synthesis of Fluorineazo-Salicylaldehyde Thiosemicarbazone Derivatives

FENG Fu1*, HU Wei-Bing1, LIU Hong-Xia1, NIE Xiang-Liang1, YU Ai-Nong1   

  1. (1.School of Chemistry and Environmental Engineering,Hubei Institute for Nationalities,Enshi 445000;
    2.School of Environmental Engineering,Huangshi Institute of Technology,Huangshi)
  • Received:2009-02-10 Revised:2009-06-23 Published:2010-02-10 Online:2010-02-10

PDF

1053

被引次数

12 | 2

摘要：

以芴、水杨醛和氨基芳基硫脲为原料合成了一系列新型芴三偶氮基水杨醛缩氨基芳基硫脲衍生物,其结构经IR、1H NMR、MS和元素分析测试技术确证。 经平皿油菜生根实验表明，该类化合物在低浓度下对油菜生根显示促进作用,高浓度下促进作用小或显示抑制作用,对油菜生根的调节作用与硫脲的苯取代基上的取代基性质有关。

关键词: 三氨基芴, 水杨醛, 三偶氮基水杨醛缩氨基芳基硫脲衍生物, 植物生长调节活性, 合成

Abstract:

A series of novel fluorenetriazosalicylaldehyde thiosemicarbazone derivatives were synthesized by reaction of fluorene, salicylaldehyde with thiosemicarbazone, and their structures were confirmed by IR, 1H NMR, MS and elemental analysis. The utensil rape rooting tests show that all the compounds have good accelerating effects on rape rooting at a low concentration, but have inhibitory or low accelerating effects on rape rooting at a high concentration. The effect on rape rooting is related to the property of substituent group.

Key words: triaminofluorene,salicylaldehyde, fluoreneazosalicylaldehyde thiosemicarbazone, effect of plant growth, synthesis

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