Chinese Journal of Applied Chemistry ›› 2023, Vol. 40 ›› Issue (11): 1518-1530.DOI: 10.19894/j.issn.1000-0518.230158
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Feng WEI1,2, Hai-Dong XING1, Zi-Yuan XIU1, De-Feng XING2, Xiao-Jun HAN1()
Received:
2023-05-30
Accepted:
2023-10-16
Published:
2023-11-01
Online:
2023-12-01
Contact:
Xiao-Jun HAN
About author:
hanxiaojun@hit.edu.cnSupported by:
CLC Number:
Feng WEI, Hai-Dong XING, Zi-Yuan XIU, De-Feng XING, Xiao-Jun HAN. Fabrication of BiOX-Based Photocatalysts and Their Applications in Energy Conversion[J]. Chinese Journal of Applied Chemistry, 2023, 40(11): 1518-1530.
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URL: http://yyhx.ciac.jl.cn/EN/10.19894/j.issn.1000-0518.230158
Photocatalyst | Preparation method | Modification strategy | Reaction condition (Light resource) | Photocatalytic performance | Ref. |
---|---|---|---|---|---|
BiOBr nanosheet arrays | Solvothermal method | Morphology regulation | 500 W Xenon lamp (λ≥400 nm) | Removal of ciprofloxacin hydrochloride (91.4%) | [ |
Hollow porous BiOCl microspheres | Spray solution combustion method | Morphology regulation | 150 W Halogen lamp (λ≥400 nm) | Removal of rhodamine B (98%) | [ |
Ultrathin 2D BiOX NSs | Two-phase method | Morphology regulation | 300 W Xenon lamp (λ≥420 nm) | Removal of rhodamine B (96%) Removal of methyl orange (39%) O2 evolution (445.6 μmol/(g·h)) | [ |
Ni-doped BiOCl | Solvothermal method | Transition metal ion doping | Visible light (λ>420 nm) | Removal of rhodamine B (97%) | [ |
B-doped Bi3O4Cl NSs | Solvothermal method | Non-metal ion doping | 300 W Xenon lamp (λ>420 nm) | Removal of bisphenol A (~94%) Removal of ciprofloxacin (92.3%) | [ |
Ultrathin BiOX NSs (X=Cl, Br) | Laser irradiation | O vacancy defect | 500 W Xenon lamp (λ≥420 nm) | Removal of rhodamine B (BiOCl: 93.6%; BiOBr: 92.1%) | [ |
BiOX (X=F, Cl, Br, I) | Hydrothermal method and chemical precipitation method | O vacancy defect | 300 W Xenon lamp | Reduction of CO2 (CO: 21.6 μmol/(g·h); CH4 1.2 μmol/(g·h)) | [ |
Bi-Nb-BiOCl | Solvothermal method | O vacancy defect | 300 W Xenon lamp (λ≥420 nm) | Removal of rhodamine B (97%) Removal of tetracycline (~70%) | [ |
p-BiOBr/n-TiO2 nanofibers | Electrospinning and solvothermal method | p-n heterojunction | 50 W Mercury lamp | Removal of rhodamine B (89%) Removal of methyl orange (~95%) | [ |
BiOX(X=Cl, Br)-Au-CdS | Solvothermal method and photodeposition | All-solid-state Z-scheme | 300 W Xenon lamp (AM 1.5 filter) | Removal of rhodamine B (100%) | [ |
BiOBr/BiOIO3 | Solvothermal method | Direct Z-scheme | 300 W Xenon lamp (λ≥420 nm) | Removal of mercury (90.25%) | [ |
BiOX (X=Cl, Br, I) | Chemical precipitation method | Selective facet | 300 W Xenon lamp (λ≥400 nm) | Removal of rhodamine B (95%) | [ |
Table 1 Summary of typical modification strategies based on BiOX and photocatalytic activities
Photocatalyst | Preparation method | Modification strategy | Reaction condition (Light resource) | Photocatalytic performance | Ref. |
---|---|---|---|---|---|
BiOBr nanosheet arrays | Solvothermal method | Morphology regulation | 500 W Xenon lamp (λ≥400 nm) | Removal of ciprofloxacin hydrochloride (91.4%) | [ |
Hollow porous BiOCl microspheres | Spray solution combustion method | Morphology regulation | 150 W Halogen lamp (λ≥400 nm) | Removal of rhodamine B (98%) | [ |
Ultrathin 2D BiOX NSs | Two-phase method | Morphology regulation | 300 W Xenon lamp (λ≥420 nm) | Removal of rhodamine B (96%) Removal of methyl orange (39%) O2 evolution (445.6 μmol/(g·h)) | [ |
Ni-doped BiOCl | Solvothermal method | Transition metal ion doping | Visible light (λ>420 nm) | Removal of rhodamine B (97%) | [ |
B-doped Bi3O4Cl NSs | Solvothermal method | Non-metal ion doping | 300 W Xenon lamp (λ>420 nm) | Removal of bisphenol A (~94%) Removal of ciprofloxacin (92.3%) | [ |
Ultrathin BiOX NSs (X=Cl, Br) | Laser irradiation | O vacancy defect | 500 W Xenon lamp (λ≥420 nm) | Removal of rhodamine B (BiOCl: 93.6%; BiOBr: 92.1%) | [ |
BiOX (X=F, Cl, Br, I) | Hydrothermal method and chemical precipitation method | O vacancy defect | 300 W Xenon lamp | Reduction of CO2 (CO: 21.6 μmol/(g·h); CH4 1.2 μmol/(g·h)) | [ |
Bi-Nb-BiOCl | Solvothermal method | O vacancy defect | 300 W Xenon lamp (λ≥420 nm) | Removal of rhodamine B (97%) Removal of tetracycline (~70%) | [ |
p-BiOBr/n-TiO2 nanofibers | Electrospinning and solvothermal method | p-n heterojunction | 50 W Mercury lamp | Removal of rhodamine B (89%) Removal of methyl orange (~95%) | [ |
BiOX(X=Cl, Br)-Au-CdS | Solvothermal method and photodeposition | All-solid-state Z-scheme | 300 W Xenon lamp (AM 1.5 filter) | Removal of rhodamine B (100%) | [ |
BiOBr/BiOIO3 | Solvothermal method | Direct Z-scheme | 300 W Xenon lamp (λ≥420 nm) | Removal of mercury (90.25%) | [ |
BiOX (X=Cl, Br, I) | Chemical precipitation method | Selective facet | 300 W Xenon lamp (λ≥400 nm) | Removal of rhodamine B (95%) | [ |
Application | Photocatalyst | Modification strategy | Functions | Light source | Product yield rate/(μmol·h-1·g-1) and selectivity | Ref. |
---|---|---|---|---|---|---|
Water splitting for H2 production | BiOBr-(001) BiOBr-(010) | High exposure of crystal face | Enhancing spatial separation of electron and hole pairs | 300 W Xenon lamp | H2: 16.12 (100%) H2: 8.69 (100%) | [ |
BiOBr/C | Schottky junction/OVs | Enhancing spatial separation of electron and hole pairs | 150 W Xenon lamp (λ≥420 nm) | H2: 2 850 (100%) | [ | |
BiOCl/CuFe2O4 | Z-scheme heterojunction | Enhancing spatial separation of electron and hole pairs/Improving reducibility of photo-induced electrons | 250 W Xenon lamp | H2: 740 (100%) | [ | |
CO2 reduction | Ultrathin BiOCl nanosheets | Morphology regulation | Regulating conduction band/Improving migration of photo-induced carriers | 300 W Xenon lamp | CO: 21.36 (~100%) CH4: trace | [ |
BiOCl atomic layers | Exposing VDWG/Forming defect of VDWG-Bi-VOs-Bi | Enhancing separation of electron and hole pairs/Promoting activation of CO2, cleavage of *COOH and desorption of *CO | 300 W Xenon lamp (λ≥400 nm) | CO: 188.2 (≥97.4%) H2: <5 (<2.6%) | [ | |
PVP-BiOBr | PVP coordination/OVs defect | Increasing local electron density/Promoting adsorption and activation of CO2 | 300 W Xenon lamp (200 mW/cm2) | CO: 263.2 (98.8%) CH4: 3.3 (1.2%) | [ | |
BiOCl/Bi2WO6 | Ⅱ-type heterojunction | Promoting CO2 and CHO* adsorption and enhancing migration and separation of carriers by built-in electric field | 300 W Xenon lamp (AM 1.5 G, 100 mW/cm2) | CH4: 6.63 (82.9%) CO+H2: 1.37 (17.1%) | [ | |
NH3 synthesis | BiOCl NSs-Fe | Fe doping/OVs by light irradiation | Promoting adsorption and activation of N2 | 300 W Xenon lamp | NH3: 1 022 (100%) | [ |
Bi5O7Br-40 | Regulating Bi contents/morphology | Promoting activation of N2 by OVs/Increasing specific surface area | 300 W Xenon lamp (200~800 nm) | NH3: 12 720 (100%) | [ | |
Bi2Sn2O7/BiOBr | S-scheme heterojunction | Enhancing migration and separation of photo-induced carriers to maintain the high reducibility of conduction band | 300 W Xenon lamp | NH3: 459.04 (100%) | [ |
Table 2 Summary of modifications and their functions of BiOX-based photocatalysts and the applications in energy conversion
Application | Photocatalyst | Modification strategy | Functions | Light source | Product yield rate/(μmol·h-1·g-1) and selectivity | Ref. |
---|---|---|---|---|---|---|
Water splitting for H2 production | BiOBr-(001) BiOBr-(010) | High exposure of crystal face | Enhancing spatial separation of electron and hole pairs | 300 W Xenon lamp | H2: 16.12 (100%) H2: 8.69 (100%) | [ |
BiOBr/C | Schottky junction/OVs | Enhancing spatial separation of electron and hole pairs | 150 W Xenon lamp (λ≥420 nm) | H2: 2 850 (100%) | [ | |
BiOCl/CuFe2O4 | Z-scheme heterojunction | Enhancing spatial separation of electron and hole pairs/Improving reducibility of photo-induced electrons | 250 W Xenon lamp | H2: 740 (100%) | [ | |
CO2 reduction | Ultrathin BiOCl nanosheets | Morphology regulation | Regulating conduction band/Improving migration of photo-induced carriers | 300 W Xenon lamp | CO: 21.36 (~100%) CH4: trace | [ |
BiOCl atomic layers | Exposing VDWG/Forming defect of VDWG-Bi-VOs-Bi | Enhancing separation of electron and hole pairs/Promoting activation of CO2, cleavage of *COOH and desorption of *CO | 300 W Xenon lamp (λ≥400 nm) | CO: 188.2 (≥97.4%) H2: <5 (<2.6%) | [ | |
PVP-BiOBr | PVP coordination/OVs defect | Increasing local electron density/Promoting adsorption and activation of CO2 | 300 W Xenon lamp (200 mW/cm2) | CO: 263.2 (98.8%) CH4: 3.3 (1.2%) | [ | |
BiOCl/Bi2WO6 | Ⅱ-type heterojunction | Promoting CO2 and CHO* adsorption and enhancing migration and separation of carriers by built-in electric field | 300 W Xenon lamp (AM 1.5 G, 100 mW/cm2) | CH4: 6.63 (82.9%) CO+H2: 1.37 (17.1%) | [ | |
NH3 synthesis | BiOCl NSs-Fe | Fe doping/OVs by light irradiation | Promoting adsorption and activation of N2 | 300 W Xenon lamp | NH3: 1 022 (100%) | [ |
Bi5O7Br-40 | Regulating Bi contents/morphology | Promoting activation of N2 by OVs/Increasing specific surface area | 300 W Xenon lamp (200~800 nm) | NH3: 12 720 (100%) | [ | |
Bi2Sn2O7/BiOBr | S-scheme heterojunction | Enhancing migration and separation of photo-induced carriers to maintain the high reducibility of conduction band | 300 W Xenon lamp | NH3: 459.04 (100%) | [ |
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