Determination of the Chemical Constituents in Aqueous Alcohol Extract of Sibiraea Angustata(Rehd.) Leaf Hand-Mazz.

doi:10.3724/SP.J.1095.2013.30135

Chinese Journal of Applied Chemistry

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Determination of the Chemical Constituents in Aqueous Alcohol Extract of Sibiraea Angustata(Rehd.) Leaf Hand-Mazz.

YAN Zhihui^1,2, JIANG Ke³, CHEN Lishu¹, ZHU Tongfei^1*, CHEN Zhu¹, YANG Yongjian², WANG Dacheng⁴

(1.Chongqing Medical and Pharmaceutical College,Chongqing 401331,China;
2.Pharmaceutical College of Lanzhou University,Lanzhou 730000,China;
3.No.324 Hospital of PLA,Chongqing 400020,China;
4.College of Animal Science and Veterinary Medicine,Jilin University,Changchun 130062,China)

Received:2013-03-18 Revised:2013-04-13 Published:2014-02-10 Online:2014-02-10

Abstract

Abstract: To determine the chemical constituents from Sibiraea angustata(Rehd.) Hand-Mazz, its 80% ethanol extract was isolated and purified by chromatograph over silica gel, Sephadex LH-20 and HPLC, etc. Nine compounds were isolated and identified as hyperoside(Ⅰ), quercetin(Ⅱ), rutin(Ⅲ), quercetin-3-O-β-D-glucopyranoside(Ⅳ), catechin(Ⅴ), vanillic acid(Ⅵ), arbutin(Ⅶ), isoferulic acid(Ⅷ), daucosterol(Ⅸ). Their chemical structures were determined by chemical methods, NMR spectral data. Compounds Ⅰ~Ⅲ and Ⅴ~Ⅶ were isolated from the leaves of Sibiraea angustata(Rehd.) Hand-Mazz. for the first time.

Key words: Sibiraea angustata(Rehd.) Hand-Mazz., chemical constituent, flavonoids, isolation, identfication

CLC Number:

O629.9

YAN Zhihui1,2, JIANG Ke3, CHEN Lishu1, ZHU Tongfei1*, CHEN Zhu1, YANG Yongjian2, WANG Dacheng4. Determination of the Chemical Constituents in Aqueous Alcohol Extract of Sibiraea Angustata(Rehd.) Leaf Hand-Mazz.[J]. Chinese Journal of Applied Chemistry, DOI: 10.3724/SP.J.1095.2013.30135.

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Determination of the Chemical Constituents in Aqueous Alcohol Extract of Sibiraea Angustata(Rehd.) Leaf Hand-Mazz.

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