Studies of Solid Polymer ElectrolytesⅠ .Synthesis and Characterization of A Novel Comblike Copolymer with Oligo-Oxyethylene Side Chains

Chinese Journal of Applied Chemistry ›› 1994, Vol. 0 ›› Issue (6): 41-44.

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Studies of Solid Polymer ElectrolytesⅠ .Synthesis and Characterization of A Novel Comblike Copolymer with Oligo-Oxyethylene Side Chains

Ding Liming, Lin Yunqing, Qi Li, Zhou Zinan, Wang Fosong

Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, ChangChun 130022

Received:1993-11-11 Revised:1994-07-14 Published:1994-12-10 Online:1994-12-10

Abstract

Abstract: A comblike polymer based on methyl vinyl ether/maleic anhydride copolymer backbone and with oligo-oxyetl1ylene side chins was synthesized for the first time. A twostep esterification has been carried out for polymer synthesis:reacting maleic anhydride with PEGME in methylethyl ketone at 80℃ for 24 hurs and then reacting the product obtained with methanol in the presence of p-toluene sulfonic acid at 60℃ for 24 hours.The structure of the product was confirmed by IR,¹³C NMR and elemental analysis.

Key words: methyl vinyl etherlmaleic anhydride copolymer, polyethyleneglycol monomethy-lester, polyetl1yleneglycol carboxylate, comblike polymer, synthesis

Ding Liming, Lin Yunqing, Qi Li, Zhou Zinan, Wang Fosong. Studies of Solid Polymer ElectrolytesⅠ .Synthesis and Characterization of A Novel Comblike Copolymer with Oligo-Oxyethylene Side Chains[J]. Chinese Journal of Applied Chemistry, 1994, 0(6): 41-44.

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Studies of Solid Polymer ElectrolytesⅠ .Synthesis and Characterization of A Novel Comblike Copolymer with Oligo-Oxyethylene Side Chains

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