An Improved Method for Oxotitanium Phthalocyanine Preparation

Chinese Journal of Applied Chemistry ›› 1994, Vol. 0 ›› Issue (1): 72-75.

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An Improved Method for Oxotitanium Phthalocyanine Preparation

Wang Zhuting, Lu Kaijuan, Wang Xiaojun, Bai Fenglian

Institute of Chemistry, Chinese Academy of Sciemces, Beijing 100080

Received:1992-12-30 Revised:1993-05-04 Published:1994-02-10 Online:1994-02-10

Abstract

Abstract: Oxotitanium phthalocyanine was synthesized from phthalonitrile and titanium te-trachloride in bicyclohexyl.It is much more convenient to separate and purify the productsby using bicyclohexyl as a solvent. Five polymorphs were obtained and characterized by X-ray powder diffractometry and FTIR spectroscopy. The absorption spectra of the poly-morphs in silicone rubbers were recorded.

Key words: oxotitanium phthalocyanine, synthesis, crystal form, organic photoconductor

Wang Zhuting, Lu Kaijuan, Wang Xiaojun, Bai Fenglian. An Improved Method for Oxotitanium Phthalocyanine Preparation[J]. Chinese Journal of Applied Chemistry, 1994, 0(1): 72-75.

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An Improved Method for Oxotitanium Phthalocyanine Preparation

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