中华医学超声杂志

应用化学 ›› 1995, Vol. 0 ›› Issue (1): 9-12.

• 研究论文 • 上一篇    下一篇

Wittig反应的研究XXI．ω-唑烯类杀菌剂的合成

丁明武1, 石德清1, 肖文精1, 黄文芳1, 吴田捷2   

  1. 1. 华中师范大学有机合成研究所, 武汉 430070;
    2. 华中师范大学分析测试中心, 武汉
  • 收稿日期:1994-04-07 修回日期:1994-07-18 出版日期:1995-02-10 发布日期:1995-02-10
  • 基金资助:
    湖北省自然科学基金资助课题

Studies on the Wittig Reaction XXI. Synthesis of ω-Azolylalkenes

Ding Mingwu1, Shi Deqing1, Xiao Wenjing1, Huang Wenfang1, Wu Tianjie2   

  1. 1. Institute of Organic Synthesis, Central China Normal University, Wuhan 430070;
    2. Center of Analysis and Testing, Central China Normal University, Wuhan
  • Received:1994-04-07 Revised:1994-07-18 Published:1995-02-10 Online:1995-02-10

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摘要： 用相转移催化Wittig反应由1,4-二溴丁烷和三苯瞬合成了ω-溴代烯类化合物,并由此制得了15种ω-唑烯类化合物,并对部分化合物进行了杀菌活性测定.

关键词: 相转移wittig反应, ω－唑烯, 合成, 杀菌活性

Abstract: Fifteen ω-azolylalkenes have been synthesized via phase transfer catalyzed WittigredctiOn from ω-bromoalkenes,which were obtained from 1,4-dibromobutane and triphenylphosphine. The compounds have been characterized by IR,1H NMR and MS.Some com-pounds were examined on their fungicidal activities.

Key words: phase transfer catalytic Wittig reaction, ω-azolylalkene, synthesis, fungicide

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