A Least Square Estimation Based Quartz Crystal Microbalance Resonant Frequency Detection Method

doi:10.11944/j.issn.1000-0518.2019.01.180321

Chinese Journal of Applied Chemistry ›› 2019, Vol. 36 ›› Issue (1): 114-119.DOI: 10.11944/j.issn.1000-0518.2019.01.180321

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A Least Square Estimation Based Quartz Crystal Microbalance Resonant Frequency Detection Method

LIU Zhenbang^a^b,MA Yingming^a,WANG Wei^a,HAN Dongxue^a,BAO Yu^a,DONG Xiandui^a^*()

^aEngineering Laboratory for Modern Analytical Techniques,c/o State Key Laboratory of Electroanalytical Chemistry,Changchun Institute of Applied Chemistry,Chinese Acdemy of Sciences,Changchun 130022,China
^bUniversity of Chinese Academy of Sciences,Beijing 100049,China

Received:2018-09-29 Accepted:2018-10-10 Published:2019-01-01 Online:2019-01-04
Contact: DONG Xiandui

Abstract

Abstract:

The impedance analysis quartz crystal microbalance has many advantages such as wide application range and more parameters, but the resonance frequency of the quartz crystal obtained by the impedance analysis method takes a long time and has poor real-time performance. In response to this problem, we analyzed the process of data fitting when using the least squares method and proposed a fast detection method for quartz crystal resonant frequency measurement. By adjusting the data coordinate system, the calculation time used for the fitting process reduced obviously. The new method was verified by experiments, compared with the traditional least squares method, the efficiency of the algorithm for calculating the resonant frequency was improved by four times, and the calculation accuracy was higher. It means the new method has high practical value.

Key words: quartz crystal microbalance, least squares, resonant frequency

LIU Zhenbang, MA Yingming, WANG Wei, HAN Dongxue, BAO Yu, DONG Xiandui. A Least Square Estimation Based Quartz Crystal Microbalance Resonant Frequency Detection Method[J]. Chinese Journal of Applied Chemistry, 2019, 36(1): 114-119.

References

[1]	Sauerbrey G.Verwendung Von Schwingquarzen Zur Wagung Dunner Schichten und Zur Mikrowagung[J]. Z Phys A Hadrons Nuclei,1959,155(2):206-222.
[2]	Kanazawa K K,Gordon J G.Frequency of a Quartz Microbalance in Contact with Liquid[J]. Anal Chem,1985,57(8):1770-1771.
[3]	Rodahl M.Simultaneous Frequency and Dissipation Factor QCM Measurements of Biomolecular Adsorption and Cell Adhesion[J]. Faraday Discuss,1997,107:229-246.
[4]	Rodahl M,Kasemo B.Frequency and Dissipation-Factor Responses to Localized Liquid Deposits on a QCM Electrode[J]. Sens Actuators B,1996,37(1):111-116.
[5]	Rodahl M,Kasemo B.A Simple Setup to Simultaneously Measure the Resonant Frequency and the Absolute Dissipation Factor of a Quartz Crystal Microbalance[J]. Rev Sci Instrum,1996,67(9):3238-3241.
[6]	Rodahl M,Höök F,Kasemo B.QCM Operation in Liquids:An Explanation of Measured Variations in Frequency and Q Factor with Liquid Conductivity[J]. Anal Chem,1996,68(13):2219-2227.
[7]	Frost R,J nsson G E,Chakarov D,et al. Graphene Oxide and Lipid Membranes:Interactions and Nanocomposite Structures[J]. Nano Lett,2012,12(7):3356-3362.
[8]	Jin J,Jiang W,Yin J,et al. Plasma Proteins Adsorption Mechanism on Polyethylene-Grafted Poly(ethylene glycol) Surface by Quartz Crystal Microbalance with Dissipation[J]. Langmuir,2013,29(22):6624-6633.
[9]	Alassi A,Benammar M,Brett D.Quartz Crystal Microbalance Electronic Interfacing Systems:A Review[J]. Sensors,2017,17(12):2799-2840.
[10]	LIU Zhenbang,MA Yingming,HAN Dongxue,et al. Development of a Novel Broadband Adaptive Electrochemical Quartz Crystal Microbalance with Dissipation Monitoring[J]. Chinese J Anal Chem,2018,46(8):1171-1174(in Chinese). 刘振邦,马英明,韩冬雪,等. 新型耗散型电化学石英晶体微天平的研制[J]. 分析化学,2018,46(8):1171-1174.
[11]	Manuel K,Lukas T,Jasmina S,et al. Broadband 120 MHz Impedance Quartz Crystal Microbalance(QCM) with Calibrated Resistance and Quantitative Dissipation for Biosensing Measurements at Higher Harmonic Frequencies[J]. Biosensors,2016,6(2):23-26.
[12]	Láng G G,Ujvári M,Horányi G. New EQCM, Voltammetric and Radiotracer Evidences Proving the Role of Cu+ Ions in the Behavior of the Cu2+-Cu System[J]. J Electroanal Chem,2002,522(2):179-188.

A Least Square Estimation Based Quartz Crystal Microbalance Resonant Frequency Detection Method

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