Rapid Determination of Total Phthalic Acid Esters by Fluorescence Spectrometry

doi:10.11944/j.issn.1000-0518.2015.01.140100

Chinese Journal of Applied Chemistry ›› 2015, Vol. 32 ›› Issue (1): 118-122.DOI: 10.11944/j.issn.1000-0518.2015.01.140100

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Rapid Determination of Total Phthalic Acid Esters by Fluorescence Spectrometry

CAI Qihong^*, WU Yuanyuan, LIN Jiangwei

Pharmaceutical and Medical Technology College of Putian University,Putian,Fujian 351100,China

Received:2014-03-28 Revised:2014-06-23 Published:2015-01-06 Online:2015-01-06
Contact: Corresponding author:CAI Qihong, professor; Tel/Fax:0594-2784947; E-mail:cqh118@163.com; Research interests:molecular luminescence analysis
Supported by:
Supported by the Key Project of Fujian Provincial Science and Technology Program(No.2011Y0048), the Fujian Provincial Undergraduate Training Program for Innovation and Entrepreneurship(No.CXCY1221), the Science and Technology Project of Putian(No.2009S02(2))

Abstract

Abstract:

A fluorescence method for phthalic acid esters determination has been developed based on enhanced fluorescence intensity of phthalic acid esters in concentrated sulfuric acid. The fluorescence intensity of the system has a linear relationship with phthalic acid esters concentration in the range of 5.00~600 μg/L with the detection limit of 0.57 μg/L. The recovery is in the range of 91.6%~105.1%. This method is simple, rapid and sensitive, and has a wide linear range. It has been successfully applied to determine the total phthalic acid esters in plastic cups and polyvinyl chloride pipe with satisfying results.

Key words: phthalic acid esters, fluorescence spectrometry, plastic cup, polyvinyl chloride pipe

CLC Number:

O657.3

CAI Qihong, WU Yuanyuan, LIN Jiangwei. Rapid Determination of Total Phthalic Acid Esters by Fluorescence Spectrometry[J]. Chinese Journal of Applied Chemistry, 2015, 32(1): 118-122.

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Rapid Determination of Total Phthalic Acid Esters by Fluorescence Spectrometry

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