Synthesis and Characterization of Poly(aryl Ether Sulfone Ether Ketone Ketone) Containing Naphthalene Links

Chinese Journal of Applied Chemistry ›› 1998, Vol. 0 ›› Issue (5): 47-49.

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Synthesis and Characterization of Poly(aryl Ether Sulfone Ether Ketone Ketone) Containing Naphthalene Links

Sheng Shouri, Cai Mingzhong, Song Caisheng

Department of Chemistry, Jiangxi Normal University, Nanchang 330027

Received:1997-11-23 Revised:1998-04-24 Published:1998-10-10 Online:1998-10-10

Abstract

Abstract: 4,4'-bis(β-naphthoxy)diphenylsulfone(BNODPS) was synthesized by reaction of β-naphthol with bis(4-chlorophenyl) sulfone in DMSO in the presence of KOH. Five polyaryl ether sulfone ether ketone ketones containing naphthalene links were prepared by low temperature solution polycondensation of BNODPS with terephthaloyl chloride(TPC), isophthaloyl chloride(IPC) and 2,5-dichloroterephthaloyl chloride(DCC), respectively in 1,2-dichlorothane and in the presence of AlCl₃ and N-methylpyrrolidone. The polymers as characterized by IR, XRD, DSC and TG techniques are non crystalline and have high glass transition temperature, good thermostability and solubitity.

Key words: polyaryl ether sulfone ether ketone ketone, synthesis, β-naphthol, aromatic diacid chloride, low temperature solution polycondensation

Sheng Shouri, Cai Mingzhong, Song Caisheng . Synthesis and Characterization of Poly(aryl Ether Sulfone Ether Ketone Ketone) Containing Naphthalene Links[J]. Chinese Journal of Applied Chemistry, 1998, 0(5): 47-49.

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Synthesis and Characterization of Poly(aryl Ether Sulfone Ether Ketone Ketone) Containing Naphthalene Links

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