Chinese Journal of Applied Chemistry ›› 1997, Vol. 0 ›› Issue (4): 94-95.

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Synthesis of 3-Methyl-4-pyrrolidinylbenzene-diazonium Zinc Chloride Double Salt

Tang Yougen, Jiang Jinzhi, Liu Chunjian   

  1. Department of Chemistry, Central South University of Technology, Changsha 410083
  • Received:1996-09-04 Revised:1997-03-31 Published:1997-08-10 Online:1997-08-10

Abstract: A novel diazo photo-sensitive reagent 3-methyl-4-pyrrolidinylbenzenediazonium zinc chloride double salt(Ⅲ) was synthesized from 2-methyl-4-nitroaniline as a starting material. The title compound and the intermediate N-(2-methyl-4-nitrophenyl)pyrrolidine(Ⅱ) were identified by UV, IR, 1H NMR spectra and elemental analysis.

Key words: methylpyrrolidinylbenzenediazonium salt, synthesis, photo-sensitive reagent