Synthesis, Characterization and Biological Activity of O-(1,2,2,2 tetrachloro)ethyl-i>O-Substituted Phenyl-Phosphoramidothionates

Chinese Journal of Applied Chemistry ›› 1997, Vol. 0 ›› Issue (2): 45-49.

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Synthesis, Characterization and Biological Activity of O-(1,2,2,2 tetrachloro)ethyl-i>O-Substituted Phenyl-Phosphoramidothionates

Li Shengbiao¹, Huang Shiqiang¹, He Liangnian², Huang Tianbao², Zhou Qingchun², Zhang Jinling²

1. Department of Chemistry, Hubei University, Wuhan 430062;
2. Institute of Organic Synthesis, Central China Normal University, Wuhan

Received:1996-08-28 Revised:1996-11-06 Published:1997-04-10 Online:1997-04-10

Abstract

Abstract: Twenty one new O-(1,2,2,2 tetrachloro)ethyl O-ubstituted phenyl phosphoramidothionates were synthesized and their structures were characterized through IR, NMR(¹H、 ³¹P)and MS. The O-(1,2,2,2 tetrachloro)ethyl thiophosphoric hydrazides could be transferred into 1,3,4,2-oxadiazaphospholanes under alkaline condition. The biological activity of the products was also tested and some compounds showed a high activity against nematode.

Key words: phosphoramidothionate, synthesis, biological activity, oxadiazaphospholane

Li Shengbiao, Huang Shiqiang, He Liangnian, Huang Tianbao, Zhou Qingchun, Zhang Jinling. Synthesis, Characterization and Biological Activity of O-(1,2,2,2 tetrachloro)ethyl-i>O-Substituted Phenyl-Phosphoramidothionates[J]. Chinese Journal of Applied Chemistry, 1997, 0(2): 45-49.

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Synthesis, Characterization and Biological Activity of O-(1,2,2,2 tetrachloro)ethyl-i>O-Substituted Phenyl-Phosphoramidothionates

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