Chinese Journal of Applied Chemistry ›› 1994, Vol. 0 ›› Issue (5): 110-111.

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Synthesis of 2,5,7,9-Tetranitro -2,5,7,9-tetrazabicyclo[4.3.0]nonan-8-one

Lu Ming, Wei Yunyang, L? Chunxu, Li Bing   

  1. Chemical Engineering School, Nanjing University of Science and Technology, Nanjing 210014
  • Received:1993-11-15 Revised:1994-05-03 Published:1994-10-10 Online:1994-10-10

Abstract: The synthesis of 2,5,7,9-tetrazabicyclo[4.3.0]nonan-8-one hydrochloride(Ⅰ) from ethylenediamine, glyoxal and urea by Mannich reaction is reported. Nitration of the compound(Ⅰ) with nitric acid in acetic anhydride gave the title compound.

Key words: azacycle, cyclonitramine, explosive, synthesis