SYNTHESIS AND CHARACTERIZATION OF SILICA ZEOLITES FROM NONALKALINE MEDIA

Chinese Journal of Applied Chemistry ›› 1993, Vol. 0 ›› Issue (2): 17-19.

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SYNTHESIS AND CHARACTERIZATION OF SILICA ZEOLITES FROM NONALKALINE MEDIA

Zhao Daqing¹, Zhang Jianguo¹, Wu Yijie¹, Pei Fengkui¹, Qiu Shilun², Pang Wenqin²

1. Changchun Institute of Applied Chemistry, Chinese, Academy of Sciences, 130022 Changchun;
2. Department of Chemistry, Jilin University, Changchun

Received:1992-01-29 Revised:1992-05-19 Published:1993-04-10 Online:1993-04-10

Abstract

Abstract: Hydrothermal crystallization of silica zeolite from nonalkaline media containing F^- anions has been investigated. The MFI type (ZSM-5) silica zeolites were obtained with tripropylamine,choline, 1,4-diazabicyclo[2,2,2]octane or piperazine as template. Silica Theta-1 and ZSM-39 were prepared using 1,6-diaminohexane and tetramethylamminum cation as template, respectively. Highly resolved ²⁹Si MAS NMR spectra of silica zeolites from nonalkaline media reveal new feature of the materials, which are indicative of the very low defect content and very high crystallinity.

Key words: silica zeolite, synthesis, characterization

Zhao Daqing, Zhang Jianguo, Wu Yijie, Pei Fengkui, Qiu Shilun, Pang Wenqin. SYNTHESIS AND CHARACTERIZATION OF SILICA ZEOLITES FROM NONALKALINE MEDIA[J]. Chinese Journal of Applied Chemistry, 1993, 0(2): 17-19.

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SYNTHESIS AND CHARACTERIZATION OF SILICA ZEOLITES FROM NONALKALINE MEDIA

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