Chinese Journal of Applied Chemistry ›› 2010, Vol. 27 ›› Issue (12): 1381-1385.DOI: 10.3724/SP.J.1095.2010.00190

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Preparation and Characterization of Emamectin Benzoate Microcapsules

LI Wei, LU Fu-Sui*, GUO Wen-Ting, LI Hui   

  1. (College of Chemistry and Materials Science,Shandong Agricultural University,Taian 271018)
  • Received:2010-03-18 Revised:2010-05-24 Published:2010-12-10 Online:2010-12-10

Abstract:

Using formaldehyde and melamine as wall materials, encapsulated emamectin benzoate-toluene microcapsules were prepared via an in-situ polymerization process. The experimental results show that well defined microcapsules with uniform particle size around 4.4 μm could be formed when the mass ratio of melamine to formaldehyde is 1∶2, core to wall is 3 to 2, using 1% mass fraction of HEC as emulsifying agent, the stirring ratio is 1000 r/min, pH value is 5.0, the temperature and heating time are 50 ℃ and 2 h, respectively. An improved photodegradation of emamectin benzoate microcapsules toward UV light could be achieved. Fourier-transform infrared spectroscopy(FT-IR) results also demonstrate the successful encapsulation of emamectin benzoate within the wall material.

Key words: emamectin benzoate, microcapsules, in-situ polymerization, preparation conditions, characterization

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