CoCuAl Hydrotalcite like Compounds:Synthesis and Use in the Catalytic Oxidation of p-CresolⅠ.Synthesis and Characterization of Hydrotalcite like Compounds

Chinese Journal of Applied Chemistry ›› 1998, Vol. 0 ›› Issue (2): 11-14.

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CoCuAl Hydrotalcite like Compounds:Synthesis and Use in the Catalytic Oxidation of p-CresolⅠ.Synthesis and Characterization of Hydrotalcite like Compounds

Liu Yumin, Zhu Kaizheng, Liu Shetian, Yie Xingkai, Wu Yue

Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022

Received:1997-09-24 Revised:1997-12-10 Published:1998-04-10 Online:1998-04-10

Abstract

Abstract: The hydrotalcite like compounds CoMAlCO₃(HTLc,M=Cu²⁺,Ni²⁺,Mn²⁺,Cr³⁺,Fe³⁺) were synthesized by coprecipitation method and characterized by XRD and IR measurements.The results showed that the interlayer H₂O and OH^- and CO₃^2- in the compounds were lost with the increase of the calcination temperature, with the structure of the compounds being changed into spinel structure. The CO₂ TPD results showed that the calcination temperature and Co/Cu ratio of the compounds had an obvious effects on the surface area and the alkalinity of the products.

Key words: CoCuAlCO₃, hydrotalcite compound, synthesis, characterization

Liu Yumin, Zhu Kaizheng, Liu Shetian, Yie Xingkai, Wu Yue. CoCuAl Hydrotalcite like Compounds:Synthesis and Use in the Catalytic Oxidation of p-CresolⅠ.Synthesis and Characterization of Hydrotalcite like Compounds[J]. Chinese Journal of Applied Chemistry, 1998, 0(2): 11-14.

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CoCuAl Hydrotalcite like Compounds:Synthesis and Use in the Catalytic Oxidation of p-CresolⅠ.Synthesis and Characterization of Hydrotalcite like Compounds

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