Preparation and Properties of Siliceous Earth/ Phenolphthalein-Based Poly(arylene ether sulfone) Composites

doi:10.11944/j.issn.1000-0518.2020.05.190346

Chinese Journal of Applied Chemistry ›› 2020, Vol. 37 ›› Issue (5): 524-530.DOI: 10.11944/j.issn.1000-0518.2020.05.190346

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Preparation and Properties of Siliceous Earth/ Phenolphthalein-Based Poly(arylene ether sulfone) Composites

GAO Limin^a,LI Lu^b,ZHOU Guangyuan^c,WANG Honghua^c,ZHU Zhongli^a^*()

^aSchool of Chemistry & Environmental Engineering,Changchun University of Science and Technology,Changchun 130022,China;
^bDivision of Energy Materials,Dalian Institute of Chemistry Physics,Dalian,Liaoning 116000,China
^cKey Laboratory of Polymer Ecomaterials,Changchun Institute of Applied Chemistry,Chinese Academy of Sciences,Changchun 130022,China

Received:2019-12-19 Accepted:2020-02-21 Published:2020-05-01 Online:2020-04-29
Contact: ZHU Zhongli
Supported by:
Supported by the Key R&D Program of Guangdong Province(No.2018B090906001)

Abstract

Abstract:

Functional modification of siliceous earth with γ-aminopropyltriethoxysilane, and functionalized siliceous earth was blended into phenolphthalein-based poly(arylene ether sulfone) (PES-C) to prepare composite materials. And its thermal properties, mechanical properties and barrier properties were characterized and analyzed. The results showed that the surface modification of γ-aminopropyltriethoxy increased the layers' pacing of siliceous earth and made the siliceous earth in the state of semi-stripping, and the doping of the surface modified siliceous earth into PES-C through solution blending was more conducive to the insertion of PES-C molecular chains. The 5% mass loss temperature (T_-5%), the T_-10% and the T_max of the composites was increased by 10.2 ℃, 10 ℃ and 3.9 ℃, respectively. In addition, the tensile strength of the composite materials increased by 8.4 MPa, the breaking elongation increased by 2.4%, and the modulus increased by 560.7 MPa. The $P_{O_{2}}$ of composites was reduced by 77.4%.

Key words: siliceous earth, phenolphthalein-based poly(arylene ether sulfone), composites, thermal properties, mechanical properties, gas barrier properties

GAO Limin, LI Lu, ZHOU Guangyuan, WANG Honghua, ZHU Zhongli. Preparation and Properties of Siliceous Earth/ Phenolphthalein-Based Poly(arylene ether sulfone) Composites[J]. Chinese Journal of Applied Chemistry, 2020, 37(5): 524-530.

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Preparation and Properties of Siliceous Earth/ Phenolphthalein-Based Poly(arylene ether sulfone) Composites

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