应用化学 ›› 2024, Vol. 41 ›› Issue (2): 190-216.DOI: 10.19894/j.issn.1000-0518.230309
• 综合评述 • 上一篇
庞子君, 覃智, 陈啊聪, 关翔鸿, 韦庚锐, 李泽敏, 黄华, 韦朝海()
收稿日期:
2023-10-09
接受日期:
2023-12-26
出版日期:
2024-02-01
发布日期:
2024-03-05
通讯作者:
韦朝海
基金资助:
Zi-Jun PANG, Zhi QIN, A-Cong CHEN, Xiang-Hong GUAN, Geng-Rui WEI, Ze-Min LI, Hua HUANG, Chao-Hai WEI()
Received:
2023-10-09
Accepted:
2023-12-26
Published:
2024-02-01
Online:
2024-03-05
Contact:
Chao-Hai WEI
About author:
cechwei@scut.edu.cnSupported by:
摘要:
污废水中的有机污染物、重金属离子和病毒性微生物等造成了严重的水环境污染,对人体健康和生态系统也造成严重威胁,有效控制污废水的风险成为保护环境和可持续发展的重要研究方向。 环境功能材料作为一类具有污染物净化效果的辅助性手段,在降低水污染风险中展现出巨大的科技潜力。 本研究探讨元素物质的选择、合成改性策略和工艺工程的优化3个尺度层面的现状与发展; 以碳元素、硅元素和金属元素为例,介绍新型功能材料的特征; 从溶剂热法、溶胶-凝胶法、共沉淀法、化学气相沉积法、绿色合成法以及表面功能化改性讨论了合成技术策略; 关于工艺工程应用方面,固定床-吸附床-流化床、电场-光场-磁场、物理-化学-生物、循环-再生-处置和协同放大效应等的产业生产/连续运行方面值得关注; 在性能、经济性、环境影响和可持续性方面进行评价,强调了安全-稳定-长效-满负荷-优化的工艺工程技术应用目标。 未来的环境功能材料发展应聚焦3D打印材料在污废水处理中的应用、智能工艺和智慧管理、群体感知和信息诊断以及场域效应和量子探针等技术方向的结合,在水质改善-材料功能挖掘-可持续循环发展方面提供新的技术领域。
中图分类号:
庞子君, 覃智, 陈啊聪, 关翔鸿, 韦庚锐, 李泽敏, 黄华, 韦朝海. 污废水中污染物去除的功能材料研究进展:元素物质-合成改性-工艺工程的尺度效应[J]. 应用化学, 2024, 41(2): 190-216.
Zi-Jun PANG, Zhi QIN, A-Cong CHEN, Xiang-Hong GUAN, Geng-Rui WEI, Ze-Min LI, Hua HUANG, Chao-Hai WEI. Recent Advances in Functional Materials for Pollutant Removal from Sewage Wastewater: Scaling Effects of Elemental Substances‑Synthetic Modification‑Process Engineering[J]. Chinese Journal of Applied Chemistry, 2024, 41(2): 190-216.
图1 (a)碳基[19-20]、(b)硅基[21-28]和(c)金属基[29-35]环境功能材料的种类
Fig.1 Types of (a) carbon-based[19-20], (b) silicon-based[21-28] and (c) metal-based[29-35] environmentally functional material
Name | Structures | Synthesis methods | Advantages | Disadvantages | Specific surface area/(m2·g-1) | Ref. |
---|---|---|---|---|---|---|
GNS | Mechanical stripping, chemical vapor deposition | High quality, large size, few defects | Small production scale, low yield | ~2 391 | [ | |
sGNS | Introduction of sulfonyl groups (—SO3H) on graphene surface | Introduction of functional groups increases chemical versatility | Complex preparation, sensitive to oxidizers | ~1 709 | [ | |
GO | Modified Hummers method | Large scale production, safe and controllable, high purity yield | Unstable oxide layer | ~2 400 | [ | |
rGO | Liquid phase reduction | Low cost, highly decentralized and controllable, environmentally friendly | Unstable reduction process | ~2 700 | [ |
表1 石墨烯及其衍生物的结构和性质
Table 1 Structure and properties of graphene and its derivatives
Name | Structures | Synthesis methods | Advantages | Disadvantages | Specific surface area/(m2·g-1) | Ref. |
---|---|---|---|---|---|---|
GNS | Mechanical stripping, chemical vapor deposition | High quality, large size, few defects | Small production scale, low yield | ~2 391 | [ | |
sGNS | Introduction of sulfonyl groups (—SO3H) on graphene surface | Introduction of functional groups increases chemical versatility | Complex preparation, sensitive to oxidizers | ~1 709 | [ | |
GO | Modified Hummers method | Large scale production, safe and controllable, high purity yield | Unstable oxide layer | ~2 400 | [ | |
rGO | Liquid phase reduction | Low cost, highly decentralized and controllable, environmentally friendly | Unstable reduction process | ~2 700 | [ |
图3 4种主要的硅基聚合物的结构通式: (a)聚硅氧烷; (b)聚硅氮烷; (c)聚硅烷; (d)聚碳硅烷
Fig.3 Structural generalizations of the four main silicone-based polymers: (a) polysiloxanes; (b) polysilazanes; (c) polysilanes; (d) polycarbosilanes
Single atom | Carriers | AOPs technologies | Reaction conditions | Pollutant species | Removal capacity/% | Active species | Ref. |
---|---|---|---|---|---|---|---|
Co | Polystyrene microsphere templates (NC?PS) | PMS | [Catalyst]=100 mg/L [PMS]0=300 mg/L [BPA]0=20 mg/L | BPA a | 100 (60 min) | 1O2 | [ |
Fe | N?doped carbon carriers (NC) | PMS | [Catalyst]=0.05 g/L [PMS]0=2 mmol/L [BPA]0=0.1 mmol/L | BPA | 100 (3 min) | ·OH, | [ |
Ag | Mesoporous g?C3N4 | Photo?PMS | [Catalyst]=0.1 g/L [PMS]0=1 mmol/L [BPA]0=20 mg/L | BPA | 98 (60 min) | [ | |
Mn | N?doped biochar (NSC) | PMS | [Catalyst]=0.5 g/L [PMS]0=1 mmol/L [ENR]0=10 mg/L | ENR b | 99 (10 min) | ·OH, | [ |
Fe | Enteromorpha carbon matrix | PDS | [Catalyst]=40 mg/L [PDS]0=0.4 mmol/L | BPS c | 100 (40 min) | ·OH, | [ |
Cu | Carbon nitride (CN) | Fenton?like | [Catalyst]=0.3 g/L [H2O2]0=30 mmol/L [MB]0=10 mg/L | MB | 93.55 (40 min) | 1O2 | [ |
Mn | N,P,S?doped carbon skeleton | Electrocatalysis | [Catalyst]=0.4 g/L [CIP]0=10 mg/L | CIP | 100 (30 min) | Mn*,1O2,H* | [ |
Mo | CNTs | Electro?Fenton(EF) | [Catalyst]=20 mg | IBU d | 98 (30 min) | ·OH, | [ |
Fe | N?doped MOFs | EF | [Catalyst]=0.1 g/L [2,4-DCP]0=0.14 mmol/L | 2,4?DCP e | 100 (90 min) | ·OH | [ |
Pt | Thiocyanate/C | EF | [Catalyst]=1.105 mg [RhB]0=20 mg/L | RhB f | 100 (7 min) | ·OH | [ |
表2 SACs在AOPs技术中的研究进展 (Continued from previous page)
Table 2 Progress of SACs in AOPs technology
Single atom | Carriers | AOPs technologies | Reaction conditions | Pollutant species | Removal capacity/% | Active species | Ref. |
---|---|---|---|---|---|---|---|
Co | Polystyrene microsphere templates (NC?PS) | PMS | [Catalyst]=100 mg/L [PMS]0=300 mg/L [BPA]0=20 mg/L | BPA a | 100 (60 min) | 1O2 | [ |
Fe | N?doped carbon carriers (NC) | PMS | [Catalyst]=0.05 g/L [PMS]0=2 mmol/L [BPA]0=0.1 mmol/L | BPA | 100 (3 min) | ·OH, | [ |
Ag | Mesoporous g?C3N4 | Photo?PMS | [Catalyst]=0.1 g/L [PMS]0=1 mmol/L [BPA]0=20 mg/L | BPA | 98 (60 min) | [ | |
Mn | N?doped biochar (NSC) | PMS | [Catalyst]=0.5 g/L [PMS]0=1 mmol/L [ENR]0=10 mg/L | ENR b | 99 (10 min) | ·OH, | [ |
Fe | Enteromorpha carbon matrix | PDS | [Catalyst]=40 mg/L [PDS]0=0.4 mmol/L | BPS c | 100 (40 min) | ·OH, | [ |
Cu | Carbon nitride (CN) | Fenton?like | [Catalyst]=0.3 g/L [H2O2]0=30 mmol/L [MB]0=10 mg/L | MB | 93.55 (40 min) | 1O2 | [ |
Mn | N,P,S?doped carbon skeleton | Electrocatalysis | [Catalyst]=0.4 g/L [CIP]0=10 mg/L | CIP | 100 (30 min) | Mn*,1O2,H* | [ |
Mo | CNTs | Electro?Fenton(EF) | [Catalyst]=20 mg | IBU d | 98 (30 min) | ·OH, | [ |
Fe | N?doped MOFs | EF | [Catalyst]=0.1 g/L [2,4-DCP]0=0.14 mmol/L | 2,4?DCP e | 100 (90 min) | ·OH | [ |
Pt | Thiocyanate/C | EF | [Catalyst]=1.105 mg [RhB]0=20 mg/L | RhB f | 100 (7 min) | ·OH | [ |
图4 材料功能化不同合成方法的一般步骤。 (a)用于合成沸石的溶剂热法[143]; (b)溶胶-凝胶法合成流程图[144]; (c)共沉淀法合成Fe3O4纳米粒子的流程图[145]; (d) CVD法制备PPTA/PPy OSN膜的示意图[146]; (e)绿色合成流程图[147]
Fig.4 General steps of different synthesis methods for material functionalization. (a) Solvothermal method used to synthesize zeolites[143]; (b) Flowchart of the sol-gel synthesis[144]; (c) Flowchart of the co-precipitation method for the synthesis of Fe3O4 nanoparticles[145]; (d) Schematic diagram of the CVD method for the preparation of PPTA/PPy OSN membranes[146]; (e) Flowchart for green synthesis[147]
Adsorbents | pH | Concentration/(g·L-1) | Adsorption capacity/(mg·g-1) | Functionalization modification | Mechanism of action | Ref. |
---|---|---|---|---|---|---|
Douglas fir pyrolysis biochar | 5.0 | 0.4 | Pb(Ⅱ) 40 Cd(Ⅱ) 16 | —OH | Electrostatic adsorption | [ |
Coal gangue ZSM?5 zeolite | N/A | 1.0 | Pb(Ⅱ) 232.6 | —OH | Ligand complexation, precipitation and ion exchange | [176 |
Sulfonated Humic acid resin | 5.0 | 0.33 | Pb(Ⅱ) 621 Cd(Ⅱ) 366 Cu(Ⅱ) 141 | —SH, CO, C—O, —OH | Ligand complexation,α interactions | [ |
RS?g?APSAN | 6.0 | 0.4 | Pb(Ⅱ) 662.9 Cu(Ⅱ) 248.8 Zn(Ⅱ) 110.1 Ni(Ⅱ) 94.9 | —NH2 | Ligand complexation | [ |
Fe3O4@SiO2?(—NH2/ —COOH) core?shell nanoparticles | 6.0 | 0.8 | Cd(Ⅱ) 84.0 Pb(Ⅱ) 166.7 Zn(Ⅱ) 80.4 | —NH2, —COOH | Electrostatic adsorption, chemisorption, ligand complexation | [ |
2,3?Dimercaptosuccinic acid/dopamine modified magnetic iron oxide nanoparticles | 6.0 | 0.33 | Pb(Ⅱ) 187.6 Cd(Ⅱ) 49.5 Cu(Ⅱ) 63.0 | —SH, —OH, —COOH | Chemisorption | [ |
Ti?based MXene (DL?Ti3C2Tx) | 5.0 | 1.0 | Pb(Ⅱ) 77 Cu(Ⅱ) 23.1 | —OH | Electrostatic adsorption, ligand complexation | [ |
Mesoporous graphitic carbon nitride (mpg?C3N4) | 4.0 | 1.0 | Th(Ⅱ) 196.1 | NC—N,—OH | Ligand complexation, pore filling | [ |
Graphene oxide?terminated amino hyperbranched polymer (GO?HBP?NH2?TEPA) | 2.0 | 0.2 | Cr(Ⅵ) 277.2 | —NH2 | Electrostatic adsorption | [ |
Graphene oxide?terminated amino hyperbranched polymer?carboxymethyl fiber (GO?HBP?NH2?CMC) | 5.0 | 0.2 | Pb(Ⅱ) 178.2 Cd(Ⅱ) 161.4 | —OH,—NH2, —COOH, —CONH— | Monolayer chemisorption, coordination complexation, ion exchange | [ |
Microporous metal?organic skeleton (MIL?125(Ti)) | N/A | 0.2 | As(Ⅲ) 40.26 As(Ⅴ) 46.34 | CO | Monolayer adsorption | [ |
Composite of carboxylated GO and MOFs (GO?COOH/MOF?808) | 5.5 | 0.5 | Pb(Ⅱ) 157.8 Cd(Ⅱ) 136.0 Co(Ⅱ) 82.4 Ni(Ⅱ) 91.0 Cu(Ⅱ) 91.5 | —OH,—COOH | Ion exchange, electrostatic adsorption, chemisorption, α interaction, coordination complexation | [ |
表3 环境功能材料对重金属的吸附性能
Table 3 Adsorption properties of environmental functional materials for heavy metals
Adsorbents | pH | Concentration/(g·L-1) | Adsorption capacity/(mg·g-1) | Functionalization modification | Mechanism of action | Ref. |
---|---|---|---|---|---|---|
Douglas fir pyrolysis biochar | 5.0 | 0.4 | Pb(Ⅱ) 40 Cd(Ⅱ) 16 | —OH | Electrostatic adsorption | [ |
Coal gangue ZSM?5 zeolite | N/A | 1.0 | Pb(Ⅱ) 232.6 | —OH | Ligand complexation, precipitation and ion exchange | [176 |
Sulfonated Humic acid resin | 5.0 | 0.33 | Pb(Ⅱ) 621 Cd(Ⅱ) 366 Cu(Ⅱ) 141 | —SH, CO, C—O, —OH | Ligand complexation,α interactions | [ |
RS?g?APSAN | 6.0 | 0.4 | Pb(Ⅱ) 662.9 Cu(Ⅱ) 248.8 Zn(Ⅱ) 110.1 Ni(Ⅱ) 94.9 | —NH2 | Ligand complexation | [ |
Fe3O4@SiO2?(—NH2/ —COOH) core?shell nanoparticles | 6.0 | 0.8 | Cd(Ⅱ) 84.0 Pb(Ⅱ) 166.7 Zn(Ⅱ) 80.4 | —NH2, —COOH | Electrostatic adsorption, chemisorption, ligand complexation | [ |
2,3?Dimercaptosuccinic acid/dopamine modified magnetic iron oxide nanoparticles | 6.0 | 0.33 | Pb(Ⅱ) 187.6 Cd(Ⅱ) 49.5 Cu(Ⅱ) 63.0 | —SH, —OH, —COOH | Chemisorption | [ |
Ti?based MXene (DL?Ti3C2Tx) | 5.0 | 1.0 | Pb(Ⅱ) 77 Cu(Ⅱ) 23.1 | —OH | Electrostatic adsorption, ligand complexation | [ |
Mesoporous graphitic carbon nitride (mpg?C3N4) | 4.0 | 1.0 | Th(Ⅱ) 196.1 | NC—N,—OH | Ligand complexation, pore filling | [ |
Graphene oxide?terminated amino hyperbranched polymer (GO?HBP?NH2?TEPA) | 2.0 | 0.2 | Cr(Ⅵ) 277.2 | —NH2 | Electrostatic adsorption | [ |
Graphene oxide?terminated amino hyperbranched polymer?carboxymethyl fiber (GO?HBP?NH2?CMC) | 5.0 | 0.2 | Pb(Ⅱ) 178.2 Cd(Ⅱ) 161.4 | —OH,—NH2, —COOH, —CONH— | Monolayer chemisorption, coordination complexation, ion exchange | [ |
Microporous metal?organic skeleton (MIL?125(Ti)) | N/A | 0.2 | As(Ⅲ) 40.26 As(Ⅴ) 46.34 | CO | Monolayer adsorption | [ |
Composite of carboxylated GO and MOFs (GO?COOH/MOF?808) | 5.5 | 0.5 | Pb(Ⅱ) 157.8 Cd(Ⅱ) 136.0 Co(Ⅱ) 82.4 Ni(Ⅱ) 91.0 Cu(Ⅱ) 91.5 | —OH,—COOH | Ion exchange, electrostatic adsorption, chemisorption, α interaction, coordination complexation | [ |
图5 (a)中试实验和(b)全规模示范示意图,(c)催化剂的失活和再生机制[216]
Fig.5 Schematic of (a) pilot experiment and (b) full-scale demonstration, (c) deactivation and regeneration mechanism of catalyst[216]
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