Synthesis, Infrared Spectra and Crystal Structures of Zinc Phthalate Complexes

Chinese Journal of Applied Chemistry ›› 1997, Vol. 0 ›› Issue (5): 98-100.

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Synthesis, Infrared Spectra and Crystal Structures of Zinc Phthalate Complexes

Sun Jutang¹, Wang Dongli¹, Zhang Keli¹, Wang Chunlin²

1. Department of Chemistry, Wuhan University, Wuhan 430072;
2. Analysis and Testing Center, Wuhan University, Wuhan

Received:1996-12-16 Revised:1997-06-16 Published:1997-10-10 Online:1997-10-10

Abstract

Abstract: The ZnPht [Pht= o-C₆H₄(CO₂)₂^2-] and double salt Zn₉K₃₀₉(OH)₅₀₅Pht_8.2·0.35H₂Pht·4H₂O were synthesized by semi solid reaction and solution reaction methods, respectively. Their infrared spectra and TG and DTA curves were measured. The crystal structures were characterized by powder X-ray diffractometry. Both are monoclinic: for ZnPht a =1.1044, b =0.9687, c =2.5949 nm, β =92.19°, for double salt a =1.7138, b =0.8343, c =1.6879 nm, β =113.35°.

Key words: benzenedicarboxylic acid, zinc, crystal structure, infrared spectrum

Sun Jutang, Wang Dongli, Zhang Keli, Wang Chunlin. Synthesis, Infrared Spectra and Crystal Structures of Zinc Phthalate Complexes[J]. Chinese Journal of Applied Chemistry, 1997, 0(5): 98-100.

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Synthesis, Infrared Spectra and Crystal Structures of Zinc Phthalate Complexes

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