N-(酰基二茂铁)苯并咪唑类化合物的合成和表征

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摘要：

将二茂铁磺酰氯或二茂铁甲酰氯和1H-苯并咪唑衍生物反应，合成了12个未见文献报道的N-(酰基二茂铁)苯并咪唑类化合物，用IR、1HNMR、元素分析和MS对其结构进行了表征。结果表明，含有活泼氢的苯并咪唑衍生物能与二茂铁酰氯生成相应的N-(酰基二茂铁)苯并咪唑衍生物,并有较好的收率。

关键词: 二茂铁酰基苯并咪唑，合成，表征

Abstract:

twelve new ferroceneacyl benzimidazoles were prepared by the reaction of ferrocenesulfonylchloride or ferrocenylcarbonylchloride with 1H-benzimidazole derivatives.The structures of as-synthesized benzimidazoles were confirmed by IR, 1H NMR, Elemental analysis and MS. The results show that the reaction of benzimidazole derivatives containing active hydrogen with ferroceneacylchloride gave ferroceneacyl benzimidazole in good yields.

Key words: ferroceneacyl benzimidazole , synthesis, characteristic

李湘广, 杨秉勤, 谷利军, 宁伟. N-(酰基二茂铁)苯并咪唑类化合物的合成和表征[J]. 应用化学, 2009, 26(10): 1184-1188.

LI Xiang-Guang, YANG Bing-Qi, GU Li-Jun, NING Wei. Synthesis and Characterization of Ferroceneacyl Benzimidazole[J]. Chinese Journal of Applied Chemistry, 2009, 26(10): 1184-1188.

N-(酰基二茂铁)苯并咪唑类化合物的合成和表征

Synthesis and Characterization of Ferroceneacyl Benzimidazole

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