Determination of Methenamine in Dried Beancurd Stick and Bean Vermicelli by Ion Chromatography

doi:10.3724/SP.J.1095.2014.40003

Chinese Journal of Applied Chemistry

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Determination of Methenamine in Dried Beancurd Stick and Bean Vermicelli by Ion Chromatography

ZHANG Sheli^1*, XU Wenjing¹, FAN Yunchang²

(1.Jiaozuo Teachers College,Jiaozuo 454000,China；
2.College of Physics and Chemistry,Henan Polytechnic University,Jiaozuo 454003,China)

Received:2014-01-06 Revised:2014-03-12 Published:2014-10-09 Online:2014-10-09
Contact: ZHANG Sheli

Abstract

Abstract: A method for the determination of banned additive, methenamine, in dried beancurd stick and bean vermicelli by ion chromatography was established. The extraction conditions and extraction solvents were optimized. Results showed a good linearity in the range of 0.10~4.0 μg/g for methenamine with the related coefficient of 0.99937. The detection limit of the proposed method for dried beancurd stick and bean vermicelli was 0.079 μg/g. Spiked recoveries were in the range of 86%~96% and the relative standard deviation was 1.9%. The proposed method is simple and rapid and can be applied to the analysis of methenamine in dried beancurd stick and bean vermicelli.

Key words: methenamine, dried beancurd stick, bean vermicelli, ion chromatography

CLC Number:

O657.7

ZHANG Sheli1*, XU Wenjing1, FAN Yunchang2. Determination of Methenamine in Dried Beancurd Stick and Bean Vermicelli by Ion Chromatography[J]. Chinese Journal of Applied Chemistry, DOI: 10.3724/SP.J.1095.2014.40003.

References

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Determination of Methenamine in Dried Beancurd Stick and Bean Vermicelli by Ion Chromatography

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