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北苍术和茅苍术挥发油成分的比较

曾志1,2*,叶雪宁1,庞世敏1,张 涛3,2,沈妙婷1   

  1. (1.华南师范大学化学与环境学院 广州 510631；
    2.Faculty of Bioresource Sciences,Akita Prefectural University,Akita 0100195,Japan；
    3.华南师范大学光电材料与技术研究所 广州 510631)
  • 收稿日期:2011-06-07 修回日期:2011-09-03 出版日期:2012-04-10 发布日期:2012-04-10
  • 通讯作者: 曾志，教授; Tel:020139310068; Fax:020139310187; E1mail:zhizeng@scnu.edu.cn; 研究方向：天然产物化学
  • 基金资助:
    广东省科技计划重大专项 ( A 301020101 )，广东省自然科学基金 ( 01142 ) 资助项目

Comparison of the Volatile Oil Components from Atractylodes chinensis (DC.) Koidz. and Atractylodes lancea (Thunb.) DC.

ZENG Zhi1,2*, YE Xuening1, PANG Shimin1, ZHANG Tao2,3, SHEN Miaoting1   

  1. (1.School of Chemistry and Environment,South China Normal University,Guangzhou 510631,China;
    2.Faculty of Bioresource Sciences,Akita Prefectural University,Akita 010-0195,Japan;
    3.Institute of Optoelectronic Materials and Technology,South China Normal University,Guangzhou 510631,China)
  • Received:2011-06-07 Revised:2011-09-03 Published:2012-04-10 Online:2012-04-10

PDF

1476

被引次数

25 | 9

摘要： 采用气相色谱-质谱联用技术分析了北苍术和茅苍术的挥发油成分，分别鉴定出47和50种化学成分，并测定了其相对含量。 采用色谱指纹图谱八强峰法和分区法，根据色谱峰的保留时间把总离子流色谱图分为5个区，比较了北苍术和茅苍术的挥发油成分。 结果表明，在总离子流色谱图Ⅳ和Ⅴ区中，从北苍术和茅苍术中均检出苍术的主要药效成分β-桉叶油醇、苍术酮和苍术素，且相对含量较高。 这表明《中国药典》将北苍术、茅苍术统称为苍术具有一定的科学性。

关键词: 北苍术, 茅苍术, 气相色谱-质谱联用, 挥发油成分

Abstract: The volatile oil components from Atractylodes chinensis(DC.) Koidz. and Atractylodes lancea(Thunb.) DC. were analyzed by GC-MS. Forty-seven and fifty components were identified, respectively, and their relative contents were determined. The volatile oil components from Atractylodes chinensis(DC.) Koidz. and Atractylodes lancea(Thunb.) DC. were further compared with each other by using the Eight Strong Peaks and Dividing Sections of the chromatographic fingerprint methods. The total ionic current chromatograms were divided into five fingerprint sections on the basis of peak retention time. The results showed that the major active-components of Rhizoma Atractylodis are β-eudesmol, atractylon and atractylodin and they were identified with higher relative content in the Ⅳ and Ⅴ sections of the total ionic current chromatograms, suggesting that it was acceptable to combine Atractylodes chinensis(DC.) Koidz. and Atractylodes lancea(Thunb.) DC together as Rhizoma Atractylodis in the Pharmacopoeia of the People′s Republic of China.

Key words: Atractylodes chinensis(DC.) Koidz., Atractylodes lancea(Thunb.) DC., gas chromatography-mass spectrometry, volatile oil components

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